Contact an Account ManagerBy-products in the derivatization of amines with the chiral reagent 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl isothiocyanate
Summary
Type: HPLC
Application #: 105600
Catalog#: 720149.46 - MN HPLC Column, Nucleosil C18, 120A, 3um, 4.6x100mm
Detection: left, UV, 228nm, right, fluorescence, excitation 228nm, emission 342nm
Conditions: eluent: acetonitrile - 50mmol/l ammonium acetate buffer pH 6.0, (55:45, v/v)
flow rate 1ml/min
Authors: Ahnoff, M. et al.
Source: J. Chromatogr. 592 (1992) 323–329
Details
Legend: Fig. 2. Separation of products of (S)- and (R)-propranolol reacted with GITC
(0.56mM propranolol racemate, 4mM GITC and 110mM triethylamine in acetonitrile,
20min at room temperature).